FTIR Stack testing method 320 and astm method d6348
Dates: October 15-16, 2015
New Jersey Department of Environmental Protection
401 E. State Street
Trenton, NJ 08625
Room: 6th Floor Conference Room – 6E002
Class Length: 2-day lecture course with hands-on equipment demonstration
INSTRUCTOR: Dr. Grant Plummer, PhD, Enthalpy Analytics, Inc.
This course will explain Standard Test Methods for Determination of Gaseous Compounds by Extractive Direct Interface Fourier Transform Infrared (FTIR) Spectroscopy, including US EPA’s Stack Testing Method 320, “Vapor Phase Organic & Inorganic Emissions by Extractive FTIR.” FTIR measurement data are used to evaluate process conditions, emissions control devices, and for determining compliance with emission standards or other applicable permits.
This field test method employs an extractive sampling system to direct stationary source effluent to an FTIR spectrometer for the identification and quantification of gaseous compounds. This test method is potentially applicable for the determination of compounds that (1) have sufficient vapor pressure to be transported to the FTIR spectrometer and (2) absorb a sufficient amount of infrared radiation to be detected.
This field test method provides near real time analysis of extracted gas samples from stationary sources. Gas streams with high moisture content may require conditioning to minimize the excessive spectral absorption features imposed by water vapor. This method also requires the preparation of a source specific field test plan. The test plan must include the following: (1) the identification of the specific target analytes (2) the known analytical interferents specific to the test facility source effluent (3) the test data quality necessary to meet the specific test requirements and (4) the results obtained from the laboratory testing.
AGENDA AND TOPICS
• Principles of FTIR including a technical explanation of FTIR measurement principles
• Overview of the FTIR stack test methods
• A comparison between the two FTIR methods
Core Material & Principles
• Applicability, interferences, limitations to use, detection levels, etc.
• Comparison to other VOC methods
• Calibration and quality assurance procedures
• Differences between makes/models of analyzers and what to look out for as well as the advantages and disadvantages of different equipment
what to look for
• What to consider in reviewing a protocol
• Some compounds don’t have standards available for spiking with, so surrogates are used. Training will include guidance on how to select the proper surrogates.
• What to look for in observing the testing, including recommended observer record-keeping
• What to look for when reviewing the data from the testing (the report)
• FTIR validation steps and what to look for regarding that in the field.
• A physical demonstration of an FTIR analyzer with hands on participant training
• Calculations – including a hands-on exercise performing appropriate calculations
• Sample vs. calibration gas temperatures, pressures, and other settings that impact results
• Tips, tricks and pitfalls
• Safety and health considerations and recommendations
• USEPA guidance and information documents, including their electronic locations (URL)
State and local agency staff from MARAMA member agencies that conduct or observe emissions source tests in order to quantify emissions and assess compliance with local, state, and federal requirements.
REGISTRATION (Class Limit – 15)
Please register on line at APTI-Learn.
Registration Deadline: September 30, 2015
NOTE: There is NO registration fee for state and local employees attending this meeting. A nominal fee will be charged for Federal employees.
Wyndham Garden Trenton (approximately 6 blocks from NJ DEP, close to train station)
1 West Lafayette Street
Trenton, NJ 08608
1-609-421-4000 or 1-800-207-4421
Hilton Garden Inn Hamilton (approximately 2 miles from NJ DEP)
800 US Highway 130
Hamilton, NJ 08690
MARAMA SUPPORT AVAILABLE
MARAMA will offer support to cover the cost of room and tax (October 14th and 15th) for up to 2 staff per MARAMA member agency. Please note that MARAMA will reimburse supported staff members the government per diem rate in Trenton, NJ of $127.00 plus tax per night or less per MARAMA’s Travel Policy with hotel receipt (http://marama.org/training-center/travel-reimbursement). Supported attendees are responsible for all incidentals and travel. Overnight support is not available to those who live within 50 miles of the course location. If additional or alternative support is needed, pre-approval is necessary and a request must come from your agency’s Air Director (or their designee) and emailed to MARAMA’s Executive Director, Susan Wierman as well as MARAMA’s Training Coordinators, Sue Dilli or Jackie Burkhardt prior to the event. A list of what type of support is needed, an estimate of additional costs and the reason for the support is essential to include.